بررسی کارپذیری آلومینیم 7075 پیرسخت شده در فرآیند ایکپ

نوع مقاله : مقاله علمی

نویسندگان
1 گروه مهندسی مکانیک، دانشگاه ملی مهارت، تهران، ایران
2 گروه مهندسی شیمی، دانشکده مهندسی، دانشگاه گرمسار، گرمسار، ایران
چکیده
آلیاژ آلومینیم 7075 به‌عنوان یک فلز پیرسختشونده، علی‌رغم خواص مطلوبی نظیر استحکام ویژه عالی، چقرمگی خوب، شکل‌پذیری نسبتاً مناسب و استحکام خستگی بالا، به دلیل تشکیل فازهای رسوبی پایدار ناشی از پیرسختی، دارای کارپذیری نسبتاً پایینی است. ارتقای کارپذیری این ماده در فرآیند پرس‌کاری در کانال‌های هم‌مقطع زاویه‌دار (ECAP) جهت بهبود خواص مکانیکی، از اهداف این تحقیق است. در این مطالعه، پس از اعمال عملیات پیرسختی طبیعی، کارپذیری این ماده به‌عنوان غلاف در بیلت دو ماده‌ای با هسته از جنس آلومینیم خالص طی فرآیند ایکپ در دمای محیط و زاویه کانال 90 درجه و در دو حالت با و بدون اعمال فشار پشتی مورد ارزیابی قرار گرفت. نتایج نشان داد که در اثر کرنش بالای وارده بعد از یک گذر ایکپ، نشانه‌های زوال در هر دو حالت به وجود آمده است؛ ولی مشاهده شد که علائم زوال ماده‌ی غلاف از وضعیت ترک‌های عمیق، تکه‌تکه‌شدگی و گسیختگی کامل در حالت بدون فشار پشتی به شرایط ترک‌های کم‌عمق و گسست قابل اغماض در حالت با فشار پشتی تقلیل پیدا کرده است. لذا می‌توان دریافت که فشار پشتی در ارتقای کارپذیری این ماده نقش مؤثری ایفا کرده است. نتایج آزمون سختی نیز نشان داد که سختی ویکرز در شرایط آنیل اولیه (103)، پیرسخت شده (129)، ایکپ بدون فشار پشتی (162) و ایکپ با فشار پشتی (178) به ترتیب به میزان 25، 57 و 73 درصد نسبت به حالت آنیل شده اولیه افزایش یافته است که این ارتقای خواص مکانیکی ناشی از اثر هم‌زمان سخت‌کاری رسوبی طی عملیات پیرسازی و اعمال تغییر شکل پلاستیکی شدید با ایکپ سرد می‌باشد.
کلیدواژه‌ها
موضوعات

عنوان مقاله English

Experimental investigation of workability of age-hardened Aluminum 7075 in ECAP process

نویسندگان English

Reza Naseri 1
Faranak Dehghani 2
1 Department of Mechanical Engineering, Technical and Vocational University (TVU), Tehran, Iran
2 Department of Chemical Engineering, Faculty of Engineering, University of Garmsar, Garmsar, Iran
چکیده English

Aluminum alloy 7075, as a Precipitation-hardenable alloys (age-hardening), despite its desirable properties such as excellent specific strength, good fracture toughness, relatively acceptable formability, and high fatigue strength, exhibits relatively low workability due to the formation of stable precipitate phases resulting from precipitation hardening. Enhancing the workability of this material during ECAP process in order to improve its mechanical properties is one of the objectives of this study. In the present investigation, after applying natural aging treatment, the workability of this material as the casing in a bi-material billet with a CP-Al core was evaluated during ECAP at room temperature, with a channel angle of 90°, under two conditions: with and without the application of back pressure. The results indicated that, due to the high imposed strain after one ECAP pass, signs of damage appeared in both conditions; however, it was observed that the damage characteristics of the casing material were reduced from deep cracks, fragmentation, and complete fracture in the condition without back pressure to shallow cracks and negligible separation in the condition with back pressure. Therefore, it can be concluded that back pressure plays an effective role in enhancing the workability of this material. The hardness test results also showed that the Vickers hardness in the initial annealed condition (103), precipitation-hardened condition (129), ECAP without back pressure (162), and ECAP with back pressure (178) increased by 25%, 57%, and 73%, respectively, compared to the initial annealed condition. This improvement in mechanical properties is attributed to the combined effect of precipitation strengthening during the natural aging treatment and the application of severe plastic deformation through cold ECAP.

کلیدواژه‌ها English

Al 7075
Natural age hardening
ECAP
Back pressure
Workability
[1] R. Santos Güemes, B. Bellón, G. Esteban Manzanares, J. Segurado, L. Capolungo, and J. Llorca, "Multiscale modelling of precipitation hardening in Al–Cu alloys: Dislocation dynamics simulations and experimental validation," Acta Materialia, Vol. 188, pp. 475-485, 2020. doi: 10.1016/j.actamat.2020.02.033
[2] M. Ebrahimi, M. H. Shaeri, R. Naseri, and C. Gode, "Equal channel angular extrusion for tube configuration of Al-Zn-Mg-Cu alloy," Materials Science and Engineering: A, Vol. 731, pp. 569-576, 2018. doi: 10.1016/j.msea.2018.06.020
[3] J. F. Jiang, W. Ying, Y. Zhang, and H. E. Zhen, "Microstructure and mechanical properties of 7075 aluminum alloy parts formed by semi-solid thixoextrusion," Transactions of Nonferrous Metals Society of China, Vol. 33, NO. 11, pp. 3235-3249, 2023. doi: 10.1016/S1003-6326(23)66189-7
[4] S. S. Li et al., "Development and applications of aluminum alloys for aerospace industry," Journal of Materials Research and Technology, Vol. 27, pp. 944-983, 2023. doi: 10.1016/j.jmrt.2023.09.062
[5] M. A. Shafei, S. J. Hosseinipour, and M. Rajabi, "Microstructural characterization of nanostructured Al-Zn-Mg-Cu alloy during mechanical alloying and subsequent annealing," Advanced Materials Research, Vol. 829, pp. 57-61, 2014. doi: 10.4028/www.scientific.net/AMR.829.57
[6] C. Sigli, F. De Geuser, A. Deschamps, J. Lépinoux, and M. Perez, "Recent advances in the metallurgy of aluminum alloys. Part II: Age hardening," Comptes Rendus Physique, Vol. 19, NO. 8, pp. 688-709, 2018. doi: 10.1016/j.crhy.2018.10.006
[7] J. K. Odusote, A. A. Adeleke, and P. A. Ajayi, "Mechanical properties and microstructure of precipitation-hardened Al-Cu-Zn alloys," International Journal of Automotive and Mechanical Engineering, Vol. 12, p. 3033, 2015. doi: 10.15282/ijame.12.2015.26.0253
[8] S. H. Lee et al., "Precipitation strengthening in naturally aged Al–Zn–Mg–Cu alloy," Materials Science and Engineering: A, Vol. 803, p. 140719, 2021. doi: 10.1016/j.msea.2020.140719
[9] E. Scharifi, U. Savaci, Z. B. Kavaklioglu, U. Weidig, S. Turan, and K. Steinhoff, "Effect of thermo-mechanical processing on quench-induced precipitates morphology and mechanical properties in high strength AA7075 aluminum alloy," Materials Characterization, Vol. 174, p. 111026, 2021. doi: 10.1016/j.matchar.2021.111026
[10] R. Z. Valiev, R. K. Islamgaliev, and I. V. Alexandrov, "Bulk nanostructured materials from severe plastic deformation," Progress in Materials Science, Vol. 45, NO. 2, pp. 103-189, 2000. doi: 10.1016/S0079-6425(99)00007-9
[11] R. Z. Valiev and T. G. Langdon, "Principles of equal-channel angular pressing as a processing tool for grain refinement," Progress in Materials Science, Vol. 51, NO. 7, pp. 881-981, 2006. doi: 10.1016/j.pmatsci.2006.02.003
[12] J. Wang et al., "An investigation of microstructural stability in an AlMg alloy with submicrometer grain size," Acta Materialia, Vol. 44, NO. 7, pp. 2973-2982, 1996. doi: 10.1016/1359-6454(95)00314-1
[13] S. Lee et al., "Influence of scandium and zirconium on grain stability and superplastic ductilities in ultrafine-grained Al–Mg alloys," Acta Materialia, Vol. 50, NO. 3, pp. 553-564, 2002. doi: 10.1016/S1359-6454(01)00384-8
[14] D. G. Morris and M. A. Muñoz Morris, "Microstructure of severely deformed Al–3Mg and its evolution during annealing," Acta Materialia, Vol. 50, NO. 16, pp. 4047-4060, 2002. doi: 10.1016/S1359-6454(02)00268-4
[15] Z. Horita, T. Fujinami, M. Nemoto, and T. G. Langdon, "Equal-channel angular pressing of commercial aluminum alloys: Grain refinement, thermal stability and tensile properties," Metallurgical and Materials Transactions A, Vol. 31, NO. 3, pp. 691-701, 2000. doi: 10.1007/s11661-000-0095-1
[16] L. J. Zheng, C. Q. Chen, T. T. Zhou, P. Y. Liu, and M. G. Zeng, "Structure and properties of ultrafine-grained Al-Zn-Mg-Cu and Al-Cu-Mg-Mn alloys fabricated by ECA pressing combined with thermal treatment," Materials Characterization, Vol. 49, NO. 5, pp. 455-461, 2002. doi: 10.1016/S1044-5803(03)00028-0
[17] Y. H. Zhao, X. Z. Liao, Z. Jin, R. Z. Valiev, and Y. T. Zhu, "Microstructures and mechanical properties of ultrafine grained 7075 Al alloy processed by ECAP and their evolutions during annealing," Acta Materialia, Vol. 52, NO. 15, pp. 4589-4599, 2004. doi: 10.1016/j.actamat.2004.06.017
[18] J. Zhang et al., "Enhanced mechanical properties in 7075 Al alloy fasteners processed by post ECAP-CU aging," Materials Today Communications, Vol. 45, p. 112274, 2025. doi: 10.1016/j.mtcomm.2025.112274
[19] J. J. Zhang et al., "Effect of pre-heat treatment and subsequent ECAP-CU on microstructure and corrosion behavior of 7075 Al alloy fasteners," Journal of Central South University, Vol. 32, NO. 7, pp. 2383-2403, 2025. doi: 10.1007/s11771-025-5462-3
[20] B. Raddad, A. Frefer, M. Abdel Rahman, and A. Tajouri, "Some aspects of workability of engineering materials," TMS2013 Supplemental Proceedings, pp. 593-600, 2013. doi: 10.1007/978-3-319-48191-3_73
[21] R. Naseri, M. Kadkhodayan, and M. Shariati, "Static mechanical properties and ductility of biomedical ultrafine-grained commercially pure titanium produced by ECAP process," Transactions of Nonferrous Metals Society of China, Vol. 27, NO. 9, pp. 1964-1975, 2017. doi: 10.1016/S1003-6326(17)60194-3
[22] R. Naseri, H. Hiradfar, M. Shariati, and M. Kadkhodayan, "A comparison of axial fatigue strength of coarse and ultrafine grain commercially pure titanium produced by ECAP," Archives of Civil and Mechanical Engineering, Vol. 18, NO. 3, pp. 755-767, 2018. doi: 10.1016/j.acme.2017.12.002
[23] R. Naseri, "Experimental evaluation of back-pressure effect on workability and mechanical properties of commercially pure titanium in cold-ECAP process," Journal of Solid and Fluid Mechanics, Vol. 12, NO. 6, pp. 67-81, 2023 (in Persian).
[24] R. Naseri, M. Kadkhodayan, and M. Shariati, "The investigation of springback of UFG commercially pure titanium in three-point bending test," Modares Mechanical Engineering, Vol. 16, NO. 11, pp. 266-276, 2017 (in Persian).
[25] P. W. J. McKenzie and R. Lapovok, "ECAP with back pressure for optimum strength and ductility in aluminium alloy 6016. Part 1: Microstructure," Acta Materialia, Vol. 58, NO. 9, pp. 3198-3211, 2010. doi: 10.1016/j.actamat.2010.02.012
[26] P. W. J. McKenzie and R. Lapovok, "ECAP with back pressure for optimum strength and ductility in aluminium alloy 6016. Part 2: Mechanical properties and texture," Acta Materialia, Vol. 58, NO. 9, pp. 3212-3222, 2010. doi: 10.1016/j.actamat.2010.02.013
[27] A. Panigrahi et al., "Effect of back pressure on material flow and texture in ECAP of aluminum," IOP Conference Series: Materials Science and Engineering, Vol. 63, NO. 1, p. 012153, 2014. doi: 10.1088/1757-899X/63/1/012153
[28] M. H. Shaeri et al., "Effect of copper tube casing on strain distribution and mechanical properties of Al-7075 alloy processed by equal channel angular pressing," The Journal of Strain Analysis for Engineering Design, Vol. 48, NO. 8, pp. 512-521, 2013. doi: 10.1177/0309324713501844
[29] R. Y. Lapovok, "The role of back-pressure in equal channel angular extrusion," Journal of Materials Science, Vol. 40, NO. 2, pp. 341-346, 2005. doi: 10.1007/s10853-005-5695-8
[30] K. Xia, J. T. Wang, X. Wu, G. Chen, and M. Gurvan, "Equal channel angular pressing of magnesium alloy AZ31," Materials Science and Engineering: A, Vol. 410-411, pp. 324-327, 2005. doi: 10.1016/j.msea.2005.08.093
[31] V. V. Stolyarov, R. Lapovok, I. G. Brodova, and P. F. Thomson, "Ultrafine-grained Al–5 wt.% Fe alloy processed by ECAP with backpressure," Materials Science and Engineering: A, Vol. 357, NO. 1-2, pp. 159-167, 2003. doi: 10.1016/S0921-5093(03)00233-7
[32] R. Naseri, M. Kadkhodayan, and M. Shariati, "An experimental investigation of casing effect on mechanical properties of billet in ECAP process," The International Journal of Advanced Manufacturing Technology, Vol. 90, NO. 9, pp. 3203-3216, 2017. doi: 10.1007/s00170-016-9634-5
[33] P. W. J. McKenzie, R. Lapovok, and Y. Estrin, "The influence of back pressure on ECAP processed AA 6016: Modeling and experiment," Acta Materialia, Vol. 55, NO. 9, pp. 2985-2993, 2007. doi: 10.1016/j.actamat.2007.01.023
[34] M. R. Roshan, S. A. J. Jahromi, and R. Ebrahimi, "Predicting the critical pre-aging time in ECAP processing of age-hardenable aluminum alloys," Journal of Alloys and Compounds, Vol. 509, NO. 30, pp. 7833-7839, 2011. doi: 10.1016/j.jallcom.2011.05.002
[35] M. H. Shaeri et al., "Microstructure and mechanical properties of Al-7075 alloy processed by equal channel angular pressing combined with aging treatment," Materials & Design, Vol. 57, pp. 250-257, 2014. doi: 10.1016/j.matdes.2013.12.053
[36] S. Sabbaghianrad and T. G. Langdon, "A critical evaluation of the processing of an aluminum 7075 alloy using a combination of ECAP and HPT," Materials Science and Engineering: A, Vol. 596, pp. 52-58, 2014. doi: 10.1016/j.msea.2013.12.062
[37] A. Fallahi, H. Hosseini Toudeshky, and S. M. Ghalehbandi, "Effect of heat treatment on mechanical properties of ECAPed 7075 aluminum alloy," Advanced Materials Research, Vol. 829, pp. 62-66, 2014. doi: 10.4028/www.scientific.net/AMR.829.62
[38] M. H. Shaeri et al., "Texture evolution of ultrafine grained Al-7075 alloy produced by ECAP," Metallurgical Engineering, Vol. 17, NO. 56, pp. 49-57, 2015 (in Persian).
[39] M. H. Shaeri et al., "Effect of equal channel angular pressing on aging treatment of Al-7075 alloy," Progress in Natural Science: Materials International, Vol. 25, NO. 2, pp. 159-168, 2015. doi: 10.1016/j.pnsc.2015.03.004
[40] S. M. Ghalehbandi, A. Fallahi Arezoodar, and H. Hosseini Toudeshky, "Influence of aging on mechanical properties of equal channel angular pressed aluminum alloy 7075," Proceedings of the Institution of Mechanical Engineers, Part B: Journal of Engineering Manufacture, Vol. 231, NO. 10, pp. 1803-1811, 2017. doi: 10.1177/0954405415626633
[41] S. Sabbaghianrad and L. Terence G, "An evaluation of the saturation hardness in an ultrafine-grained aluminum 7075 alloy processed using different techniques," Journal of Materials Science, Vol. 50, NO. 12, pp. 4357-4365, 2015. doi: 10.1007/s10853-015-9022-2
[42] S. Fritsch, M. Scholze, and M. F. X. Wagner, "Influence of thermally activated processes on the deformation behavior during low temperature ECAP," IOP Conference Series: Materials Science and Engineering, Vol. 118, NO. 1, p. 012030, 2016. doi: 10.1088/1757-899X/118/1/012030
[43] A. Esmaeili, M. H. Shaeri, M. T. Noghani, and A. Razaghian, "Fatigue behavior of AA7075 aluminium alloy severely deformed by equal channel angular pressing," Journal of Alloys and Compounds, Vol. 757, pp. 324-332, 2018. doi: 10.1016/j.jallcom.2018.04.309
[44] S. Fritsch and M. F. X. Wagner, "On the effect of natural aging prior to low temperature ECAP of a high-strength aluminum alloy," Metals, Vol. 8, NO. 1, p. 63, 2018. doi: 10.3390/met8010063
[45] M. Elhefnawey, G. L. Shuai, Z. Li, M. Nemat Alla, D. T. Zhang, and L. Li, "On achieving superior strength for Al–Mg–Zn alloy adopting cold ECAP," Vacuum, Vol. 174, p. 109191, 2020. doi: 10.1016/j.vacuum.2020.109191
[46] S. M. Ghalehbandi, A. Fallahi, and H. Hosseini Toudeshki, "Effects of post-ECAP aging on fatigue crack growth resistance of 7075 Al alloy," Iranian Journal of Science and Technology, Transactions of Mechanical Engineering, Vol. 45, NO. 3, pp. 719-725, 2021. doi: 10.1007/s40997-021-00433-7
[47] G. Xu and S. Li, "Optimization of microstructure and mechanical properties of 7075 aluminum alloy by equal channel angular pressing technology," Engineering Research Express, Vol. 6, NO. 4, p. 045419, 2024. doi: 10.1088/2631-8695/acef43
[48] C. Elibol, K. Sagir, and M. Dogan, "Effect of equal-channel angular pressing on microstructure, aging kinetics and impact behavior in a 7075 aluminum alloy," Materials Today Communications, Vol. 39, p. 108931, 2024. doi: 10.1016/j.mtcomm.2023.108931
[49] A. P. Yadav and A. K. Padap, "Effects of multi-axial compression and double-step aging on the microstructure and mechanical properties of Al alloy 7075," Proceedings of the Institution of Mechanical Engineers, Part E: Journal of Process Mechanical Engineering, p. 09544089241253671, 2024. doi: 10.1177/09544089241253671
[50] A. I. Alateyah et al., "Characterization of microstructure, crystallographic texture, corrosion behavior and mechanical properties of severely deformed AA7075 alloy," Results in Engineering, Vol. 25, p. 103749, 2025. doi: 10.1016/j.rineng.2025.103749
[51] F. Djavanroodi, M. Daneshtalab, and M. Ebrahimi, "A novel technique to increase strain distribution homogeneity for ECAPed materials," Materials Science and Engineering: A, Vol. 535, pp. 115-121, 2012. doi: 10.1016/j.msea.2012.01.052
[52] A. Jäger, V. Gärtnerova, and K. Tesař, "Microstructure and anisotropy of the mechanical properties in commercially pure titanium after equal channel angular pressing with back pressure at room temperature," Materials Science and Engineering: A, Vol. 644, pp. 114-120, 2015. doi: 10.1016/j.msea.2015.07.038
[53] R. Naseri, H. Hiradfar, M. Shariati, and M. Kadkhodayan, "Corrosion-fatigue resistance of ultrafine grain commercially pure titanium in simulated body fluid," Proceedings of the Institution of Mechanical Engineers, Part E: Journal of Process Mechanical Engineering, Vol. 237, NO. 6, pp. 2181-2191, 2023. doi: 10.1177/09544089231156701
[54] A. G. Leacock, C. Howe, D. Brown, O. G. Lademo, and A. Deering, "Evolution of mechanical properties in a 7075 Al-alloy subject to natural ageing," Materials & Design, Vol. 49, pp. 160-167, 2013. doi: 10.1016/j.matdes.2013.01.019
[55] P. Zhang, S. X. Li, and Z. F. Zhang, "General relationship between strength and hardness," Materials Science and Engineering: A, Vol. 529, pp. 62-73, 2011. doi: 10.1016/j.msea.2011.08.059
[56] E. A. El-Danaf, "Mechanical properties and microstructure evolution of 1050 aluminum severely deformed by ECAP to 16 passes," Materials Science and Engineering: A, Vol. 487, NO. 1-2, pp. 189-200, 2008. doi: 10.1016/j.msea.2007.12.072
[57] W. Abdel Aziem, A. Hamada, T. Makino, and M. A. Hassan, "Micro/Meso-scale equal channel angular pressing of Al 1070 alloy: microstructure and mechanical properties," Journal of Materials Engineering and Performance, Vol. 29, NO. 9, pp. 6201-6211, 2020. doi: 10.1007/s11665-020-04850-6
[58] M. Wroński et al., "Microstructure characteristics of ECAP processed 1050 aluminum after deformation and 5 years later," Metals and Materials International, Vol. 27, NO. 8, pp. 2720-2731, 2021. doi: 10.1007/s12540-021-00614-4
 
 

  • تاریخ دریافت 09 مرداد 1404
  • تاریخ بازنگری 25 آبان 1404
  • تاریخ پذیرش 26 آبان 1404
  • تاریخ اولین انتشار 26 آبان 1404
  • تاریخ انتشار 01 مرداد 1405